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Analysis of the volatile oil from the stem of acanthopanax senticosus (Rupr. et Maxim.) harms with several hyphenated methods of chromatography |
| Yu Wanying1, Zhang Hua2, Huang Weidong2, Chen Jiping2, Liang Xinmiao2 |
| 1.Advanced Analytical Center, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, China; 2.Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116023, China, |
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Abstract Gas chromatography/quadrupole mass spectrometry (GC/qMS), gas chromatography/Fourier transform infrared spectrometry (GC/FTIR) and gas chromatography/orthogonal acceleration time-of-flight mass spectrometry (GC/oaTOFMS) were applied to analyze the volatile oil from the stem of Acanthopanax Senticosus (Rupr. et Maxim.) Harms. Based on the mass spectra search function of GC/qMS with the aid of the discriminability of the geometrical isomer by GC/FTIR and the ability to determine the accurate mass charge ratio (m/z) by GC/oaTOFMS, 68 GC eluants were identified successfully. Compared with the results obtained by GC/qMS only, the analytical results obtained by these hyphenated methods of gas chromatography are more credible.
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Issue Date: 05 June 2006
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