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Investigation of ferroelectric properties on nanocrystalline barium titanate ceramics |
DENG Xiangyun1, LI Dejun1, WANG Xiaohui2, LI Longtu2 |
1.College of Physics and Electronic Information, Tianjin Normal University, Tianjin 300387, China; 2.State Key Lab of New Ceramics and Fine Processing, Department of Materials Science and Engineering, Tsinghua University, Beijing 100084, China; |
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Abstract Dense nanocrystalline BaTiO3 (BT) ceramics with 50 nm average grain size obtained by spark plasma sintering were investigated. The dielectric data showed a ferro para phase transition with a maximum permittivity of 1,602 at 120ºC and at 1 kHz. The polarization reversal characteristics were measured, and the typical piezoelectric hysteresis loop was recorded. The asymmetry of permanent polarization and coercive field in polarization-electric field curves were obtained and attributed to the existence of an internal electric field. The present results provide experimental evidence, indicating that if a critical grain size exists for ferroelectricity, then it is less than 50 nm for polycrystalline BT ceramics.
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Issue Date: 05 September 2007
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