Facile synthesis of magnetic iron oxide nanoparticles and their characterization

doi:10.1007/s11706-014-0249-5

Front. Mater. Sci.

2014, Vol. 8

Issue (2) : 193-198 https://doi.org/10.1007/s11706-014-0249-5

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Facile synthesis of magnetic iron oxide nanoparticles and their characterization

Sushilkumar A. JADHAV^1,^*(

),Suresh V. PATIL²

1. Department of Chemistry and NIS Center, University of Torino, 10125 Torino, Italy
2. Department of Chemistry, K.B.P. College Pandharpur affiliated to Solapur University, Solapur (MH), India

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Abstract

Magnetic iron oxide nanoparticles are synthesized by suitable modification of the standard synthetic procedure without use of inert atmosphere and at room temperature. The facile synthesis procedure can be easily scaled up and is of important from industrial point of view for the commercial large scale production of magnetic iron oxide nanoparticles. The synthesized nanoparticles were characterized by thermal, dynamic light scattering, scanning electron microscopy and transmission electron microscopy analyses.

Keywords iron oxide iron oxide nanoparticle co-precipitation

Corresponding Author(s): Sushilkumar A. JADHAV

Issue Date: 24 June 2014

Cite this article:

Sushilkumar A. JADHAV,Suresh V. PATIL. Facile synthesis of magnetic iron oxide nanoparticles and their characterization[J]. Front. Mater. Sci., 2014, 8(2): 193-198.

URL:

https://academic.hep.com.cn/foms/EN/10.1007/s11706-014-0249-5
https://academic.hep.com.cn/foms/EN/Y2014/V8/I2/193

Fig.1 Outline of set-up used for magnetite nanoparticle synthesis, pictures showing suspension of synthesized nanoparticles and their attraction towards strong magnetic field.

Fig.2 ATR-FTIR spectrum of magnetic iron oxide nanoparticles.

Fig.3 XRD pattern of the synthesized magnetic iron oxide nanoparticles and comparison with the standard diffraction pattern of magnetite nanoparticles.

Fig.4 TGA curve of magnetic iron oxide nanoparticles.

Fig.5 Histograms showing PSD of synthesized magnetite nanoparticles by intensity, volume and number distribution.

Fig.6 Zeta potential of synthesized nanoparticles.

Fig.7 SEM images of synthesized magnetite nanoparticles.

Fig.8 TEM image of synthesized magnetite nanoparticles.

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