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Synthesis, crystal structure and thermal analysis of a new stilbazolium salt crystal |
Bing TENG1,2,*( ),Weijin KONG1,2,Ke FENG1,2,Fei YOU1,2,Lifeng CAO1,2,Degao ZHONG1,2,Lun HAO1,2,Qing SUN1,2,Sander van SMAALEN3,Wenhui GONG1,2 |
1. College of Physics, Qingdao University, Qingdao 266071, China
2. Key Laboratory of Photonics Materials and Technology in Universities of Shandong, Qingdao 266071, China
3. Laboratory of Crystallography, University of Bayreuth, D-95440 Bayreuth, Germany |
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Abstract A new organic crystal of 4-N, N-dimethylamino-4′-N′-methyl-stilbazolium benzene sulfonate (DASBS) was synthesized and characterized for the first time. It is a derivative of 4-N, N-dimethylamino-4′-N′-methyl-stilbazolium tosylate (DAST) with the benzene sulfonate replacing p-toluenesulfonate. Single crystal XRD demonstrated that the crystal structure of DASBS·H2O was triclinic. The thermal analysis of this new crystal was also conducted, and the melting point was obtained to be 232°C.
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| Keywords
organic crystal
crystal growth
single crystal X-ray diffraction
thermal analysis
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Corresponding Author(s):
Bing TENG
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Online First Date: 21 April 2015
Issue Date: 23 July 2015
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