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Frontiers of Structural and Civil Engineering

ISSN 2095-2430

ISSN 2095-2449(Online)

CN 10-1023/X

Postal Subscription Code 80-968

2018 Impact Factor: 1.272

Front Struc Civil Eng    0, Vol. Issue () : 62-71    https://doi.org/10.1007/s11709-013-0192-z
RESEARCH ARTICLE
An experimental study for optimization of high range water reducing superplasticizer in self compacting concrete
Rahul DUBEY(), Pardeep KUMAR
Department of Civil Engineering, National Institute of Technology, Hamirpur 177005, India
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Abstract

Concrete is extensively used construction material in the infrastructure development industry. With increase in technical knowhow, the need of research for high performance concretes such as self-compacting concrete (SCC) has increased in the last decade. The adaptability of SCC is due to its fluidic behavior in fresh state. However, to develop SCC using indigenous materials, the lack of standardized mix design procedures is the biggest impediment. Although with the advent of chemical admixtures, it is possible to achieve concrete with high fluidity, but at the same time durability issues require more attention. To have these fresh state properties SCC mixes are typically designed with high powder contents, and chemical admixtures. Proportioning and optimization of these materials is a key issue in the mix design of SCC. This paper focuses mainly on experimental study to optimize dosages of superplasticizer for mortar of SCC and then in concrete mixture itself.

Keywords self-compacting concrete (SCC)      fresh properties      superplasticizer      optimization      compressive strength     
Corresponding Author(s): DUBEY Rahul,Email:rahulnitham0051@gmail.com   
Issue Date: 05 March 2013
 Cite this article:   
Rahul DUBEY,Pardeep KUMAR. An experimental study for optimization of high range water reducing superplasticizer in self compacting concrete[J]. Front Struc Civil Eng, 0, (): 62-71.
 URL:  
https://academic.hep.com.cn/fsce/EN/10.1007/s11709-013-0192-z
https://academic.hep.com.cn/fsce/EN/Y0/V/I/62
propertyfly ashsilica fume
(SiO2 + Al2O3 + Fe2O)% by mass92.5194
(SiO2)% by mass53.2692
MgO% by mass0.780.28
total alkali (Na2O+ K2O)% by mass0.771.12
sulphuric anhydride % by mass0.160.19
Al2O3% by mass28.650.46
Fe2O3% by mass5.611.6
Tab.1  Chemical properties of fly ash and silica fume
propertiesfine aggregatescoarse aggregates
bulk density (loose)/(kg·m-3)1681.591478.6
bulk density (compacted)/(kg·m-3)1492.531577.11
specific gravity2.62.65
water absorption/%2.041.47
fineness modulus2.405.98
Tab.2  Physical properties of fine and coarse aggregate
materialsMix 1Mix 2
OPC/(kg·m-3)400450
fly ash/(kg·m-3)125100
silica fume/(kg·m-3)3550
coarse aggregate/(kg·m-3)660800
fine aggregate/(kg·m-3)780960
Tab.3  Mix proportions for SCC
Sr. no.w/pMix 1Mix 2
d1d2dΓp/md1d2dΓp/m
11.11301201250.56251101201150.3225
21.22001801902.61120125122.50.5
31.3270265267.56.152002102053.2
41.4345330337.510.392602802706.29
51.536034035011.252953053008
Tab.4  Relative flow spread in the mixes (Results of mini slump cone test on paste)
Fig.1  (a) Geometric dimensions of mini slump cone; (b) mini slump cone apparatus
Fig.2  (a) Retained water ratio for Mix 1; (b) retained water ratio for Mix 2
trial no.w/pSP dosage/%Mix 1remarksMix 1remarks
slump flow/mmV-funnel time/sslump flow/mmV-funnel time/s
10.85βp0.80blocking0blocking
20.9βp0.80blocking0blocking
30.95βp0.80blocking0blocking
41.0βp0.80blocking0blocking
50.85βp1.012blocking0blocking
60.9βp1.017blocking0blocking
70.95βp1.019.5250blocking
81.0βp1.022210blocking
90.85βp1.211blocking11.5blocking
100.9βp1.214blocking13.6blocking
110.95βp1.21622.415.225
121.0βp1.223.5191723.4
130.85βp1.41317.612.321
140.9βp1.42014.818.218.6
150.95βp1.425.610.6optimum2116
161.0βp1.426.69.82314.7
170.85βp1.623.412.81416.3
180.9βp1.624.212.619.315
190.95βp1.6269.222.613.2
201.0βp1.6288.525.79.8optimum
210.85βp1.824.711.41512.1
220.9βp1.82710.825.111.6
230.95βp1.8298.327.310.5
241.0βp1.831.66.82910
250.85βp2.028.19.42011.6
260.9βp2.029.88.622.511
270.95βp2.031.47.52610.4
281.0βp2.036.36.2318
Tab.5  Test results for optimum volumetric w/p ratio and SP dosage in mortar
Fig.3  (a) Geometric dimensions of mini V-funnel; (b) mini V-funnel apparatus
Fig.4  (a) Flow spread from mini slump cone test; (b) flow of mortar during mini V-funnel test
Fig.5  (a) Geometric dimensions of slump cone; (b) slump cone apparatus (unit: mm)
Fig.6  (a) Geometric dimensions of V-funnel; (b)V-funnel apparatus (unit: mm)
Fig.7  (a) Geometric dimensions of L-box; (b) L-box apparatus (unit: mm)
test methodrecommended value as per EFNARC specificationsobserved value for % dosage of SP by weight of powder (Mix 1 with w/p)
1.41.61.82.02.22.42.62.83.0
slump flow(Abram’s slump cone) & T500600–750 mmin 5 s619in5.2 s665 in 4.3 s670.5 in 3.8 s690in 3.6 s714.5in 4.2 s743.5in3.2 sring ofpowder/mortar760in3.7 sring ofpowder/mortarbleeding &segregationbleeding & segregation
V-funnel(flow time)8 to 12 s12.810.79.47.87.67.16.88.18.4
L-box(h2/h1)T400/sT600/s0.8–1.01.0±0.5 s2.5±0.5 s0.742.4 s3.2 s0.821.9 s2.7 s0.861.3 s2.2 s0.910.8 s1.9 s0.930.6 s1.4 s0.95 with top layer of slurry0.4 s1.8 s0.97with top layer of slurry1.2 s2.3 sbleeding&segregation1.8 s3.1 sbleeding&segregation2.7 s3.8 s
Tab.6  Fresh properties of Mix 1
test methodrecommended value as per EFNARC specificationsobserved value for % dosage of SP by weight of powder (Mix 2 with w/p)
1.41.61.82.02.22.42.62.83.0
slump flow(Abram’s slump cone) & T50600–750 mmIn 5 s585.5in 6.7 s645in 4.8 s657.5in 4.2 s685in 3.7 s705in 4.1 s723in 3.8 s749in 3.5 s763in 3.9 sbleeding &segregation
V-funnel(flow time)8 to 12 s15 s12.7 s10.8 s10.3 s9.4 s7.6 s7.2 s8.3 s8.9 s
L-box(h2/h1)T400/sT600/s0.8-1.01.0±0.5 s2.5±0.5 s0.682.7 s3.5 s0.752.2 s3.7 s0.831.6 s2.9 s0.881.4 s2.6 s0.90.8 s1.9 s0.920.6 s1.5 s0.940.9 s2.1 stop layer of slurry1.7 s3.3 stop layer of slurry2.1 s4.5 s
Tab.7  Fresh properties of Mix 2
dosage of SPcompressive Strength after no. of water curing days for Mix 1/MPacompressive Strength after no. of water curing days for Mix 2/MPa
72856907285690
1.6%11.7023.3426.4030.90SCC not achieved
1.8%9.8021.6525.5129.7615.4526.5131.8740.60
2.0%8.2119.7822.4526.012.2922.4628.7034.50
2.2%7.3616.4118.6022.5410.3120.6325.4431.74
Tab.8  Compressive strength of SCC mixes
Fig.8  (a) Slump flow of SCC; (b) Flow of SCC during V-funnel test
Fig.9  Flow through rebar during L-box test
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