Nitrogen-doped carbon-coated hollow SnS<sub>2</sub>/NiS microflowers for high-performance lithium storage

doi:10.1007/s11706-023-0654-8

Front. Mater. Sci.

2023, Vol. 17

Issue (3) : 230654 https://doi.org/10.1007/s11706-023-0654-8

RESEARCH ARTICLE

Nitrogen-doped carbon-coated hollow SnS₂/NiS microflowers for high-performance lithium storage

Junhai Wang¹, Jiandong Zheng¹(

), Liping Gao¹, Qingshan Dai², Sang Woo Joo³(

), Jiarui Huang²(

)

¹. School of Material and Chemical Engineering, Chuzhou University, Chuzhou 239000, China
². Key Laboratory of Functional Molecular Solids of the Ministry of Education, College of Chemistry and Materials Science, Anhui Normal University, Wuhu 241002, China
³. School of Mechanical Engineering, Yeungnam University, Gyeongsan, Gyeongbuk 38541, Republic of Korea

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Abstract

Nitrogen-doped carbon-coated hollow SnS₂/NiS (SnS₂/NiS@N–C) microflowers were obtained using NiSn(OH)₆ nanospheres as the template via a solvent-thermal method followed by the polydopamine coating and carbonization process. When served as an anode material for lithium-ion batteries, such hollow SnS₂/NiS@N–C microflowers exhibited a capacity of 403.5 mAh·g⁻¹ at 2.0 A·g⁻¹ over 200 cycles and good rate performance. The electrochemical reaction kinetics of this anode was analyzed, and the morphologies and structures of anode materials after the cycling test were characterized. The high stability and good rate performance were mainly due to bimetallic synergy, hollow micro/nanostructure, and nitrogen-doped carbon layers. The revealed excellent electrochemical energy storage properties of hollow SnS₂/NiS@N–C microflowers in this study highlight their potential as the anode material.

Keywords SnS₂ NiS microflower hollow structure nitrogen-doped carbon anode lithium-ion battery

Corresponding Author(s): Jiandong Zheng,Sang Woo Joo,Jiarui Huang

Issue Date: 24 July 2023

Cite this article:

Junhai Wang,Jiandong Zheng,Liping Gao, et al. Nitrogen-doped carbon-coated hollow SnS₂/NiS microflowers for high-performance lithium storage[J]. Front. Mater. Sci., 2023, 17(3): 230654.

URL:

https://academic.hep.com.cn/foms/EN/10.1007/s11706-023-0654-8
https://academic.hep.com.cn/foms/EN/Y2023/V17/I3/230654

Fig.1 Schematic diagram of the preparation process for hollow SnS₂/NiS@N–C microflowers.

Fig.2 (a) The XRD pattern of NiSn(OH)₆ nanospheres. (b) XRD patterns of hollow SnS₂/NiS and SnS₂/NiS@N–C microflowers.

Fig.3 (a) SEM and (b) TEM images of NiSn(OH)₆ nanospheres. (c) SEM and (d) TEM images of hollow SnS₂/NiS microflowers. (e) SEM and (f) TEM images of hollow SnS₂/NiS@N–C microflowers. (g) HRTEM image and (h) SAED pattern of hollow SnS₂/NiS@N–C microflowers.

Fig.4 (a) The TGA curve of hollow SnS₂/NiS@N–C microflowers. (b) Raman spectra of hollow SnS₂/NiS and SnS₂/NiS@N–C microflowers. N₂ adsorption/desorption isotherms of (c) hollow SnS₂/NiS and (d) SnS₂/NiS@N–C microflowers (insets are the corresponding pore-size distribution curves).

Fig.5 XPS spectra of hollow SnS₂/NiS@N–C microflowers: (a) survey, (b) Ni 2p, (c) Sn 3d, (d) S 2p, (e) C 1s, and (f) N 1s spectra.

Fig.6 (a) Initial five CV curves of the hollow SnS₂/NiS@N–C microflower anode at a scan rate of 0.1 mV·s^?1. (b) Charge/discharge profiles for the 1st, 2nd, 50th, 100th, and 200th cycles at a current density of 0.2 A·g^?1. (c) Cycling performance of the hollow SnS₂/NiS@N–C microflower anode at 0.2 A·g^?1. (d) Rate performance of hollow SnS₂/NiS@N–C and SnS₂/NiS microflower anodes at various current densities. (e) Cycling performance of hollow SnS₂/NiS@N–C and SnS₂/NiS microflower anodes at 2.0 A·g^?1.

Fig.7 (a) CV curves of the hollow SnS₂/NiS@N–C microflower anode at different scan rates ranging from 0.1 to 1.0 mV·s^?1. (b) Plots of lgi versus lgv for two peaks. (c) The CV curve with the pseudocapacitive fraction shown by the red region at a scan rate of 1.0 mV·s^?1. (d) Capacitive contribution ratios at different scan rates for the hollow SnS₂/NiS@N–C microflower anode.

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